TA Instruments

AR1719-0001f

04/09/2012 18:05:45

Sample name	ASW 10 mm from base, 60 mm to top, disk 21 Provil novo medium texture REMOVED
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1719
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 18:05:45

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-31.98	5.245	-6.098	1.0000	22.4	1986	1.8622	10000	0.4873	72.17	2.3277	232.77	3.384E-3	0.0	1.0	61.000	-98.123	4.196
0.6926	12.54	0.05522	2.0120	22.4	1988	13.5421	10000	0.4880	12.64	16.928	1692.8	3.384E-3	0.0	1.0	62.012	2.1248	10.03
1.479	19.47	0.07596	2.9960	22.4	1980	27.2010	10000	0.4859	5.222	34.001	3400.1	3.383E-3	0.0	1.0	62.996	4.5373	15.58
2.056	23.13	0.08892	4.0040	22.4	1981	41.2398	10000	0.4861	3.703	51.550	5155.0	3.383E-3	0.1	1.1	64.004	6.3091	18.50
3.350	30.89	0.1084	5.0040	22.4	1982	67.7110	10000	0.4865	2.077	84.639	8463.9	3.384E-3	0.1	1.1	65.004	10.278	24.71
5.067	39.50	0.1283	6.0200	22.4	1986	107.0260	10000	0.4873	1.273	133.78	13378	3.384E-3	0.1	1.1	66.020	15.546	31.60
5.749	42.55	0.1351	7.0120	22.4	1990	126.6070	10000	0.4884	1.099	158.26	15826	3.384E-3	0.1	1.1	67.012	17.636	34.04
7.292	49.14	0.1484	7.9960	22.4	1984	165.3430	10000	0.4869	0.8216	206.68	20668	3.383E-3	0.1	1.1	67.996	22.372	39.31
9.667	57.55	0.1680	9.0040	22.4	1976	223.2280	10000	0.4849	0.5966	279.04	27904	3.384E-3	0.2	1.2	69.004	29.658	46.04
11.67	63.70	0.1832	9.9960	22.4	1972	274.8260	10000	0.4839	0.4858	343.53	34353	3.383E-3	0.2	1.2	69.996	35.807	50.96
13.74	69.66	0.1972	11.008	22.4	1972	326.1380	10000	0.4841	0.4064	407.67	40767	3.383E-3	0.2	1.2	71.008	42.153	55.73
15.51	75.13	0.2064	12.012	22.4	1961	377.3150	10000	0.4813	0.3474	471.64	47164	3.384E-3	0.2	1.2	72.012	47.575	60.10
17.21	80.52	0.2137	13.012	22.4	1971	434.8570	10000	0.4837	0.3039	543.57	54357	3.384E-3	0.2	1.2	73.012	52.789	64.42
19.57	86.44	0.2264	14.000	22.4	1974	498.6910	10000	0.4845	0.2642	623.36	62336	3.383E-3	0.2	1.2	74.000	60.040	69.15
22.46	94.61	0.2374	14.996	22.4	1953	594.2830	10000	0.4794	0.2182	742.85	74285	3.384E-3	0.2	1.2	74.996	68.899	75.69
24.81	99.92	0.2483	15.996	22.4	1966	664.6670	10000	0.4825	0.1969	830.83	83083	3.384E-3	0.3	1.3	75.996	76.119	79.93
26.95	105.7	0.2550	17.012	22.4	1945	740.7780	10000	0.4774	0.1742	925.97	92597	3.383E-3	0.3	1.3	77.012	82.683	84.54
30.09	113.7	0.2646	18.000	22.4	1930	855.6470	10000	0.4737	0.1492	1069.6	1.0696E5	3.384E-3	0.3	1.3	78.000	92.321	90.99
32.49	118.8	0.2735	19.004	22.4	1958	931.2440	10000	0.4806	0.1388	1164.1	1.1641E5	3.384E-3	0.3	1.3	79.004	99.691	95.04
34.79	124.3	0.2800	20.004	22.4	1948	1020.2200	10000	0.4780	0.1261	1275.3	1.2753E5	3.383E-3	0.3	1.3	80.004	106.73	99.40
38.51	132.3	0.2911	21.020	22.4	1943	1154.1700	10000	0.4770	0.1111	1442.7	1.4427E5	3.383E-3	0.4	1.4	81.020	118.14	105.8
41.24	137.4	0.3002	21.996	22.4	1943	1243.0601	10000	0.4770	0.1030	1553.8	1.5538E5	3.384E-3	0.4	1.4	81.996	126.52	109.9
43.35	142.8	0.3036	23.012	22.4	1934	1343.5699	10000	0.4748	0.09486	1679.5	1.6795E5	3.384E-3	0.4	1.4	83.012	133.00	114.2
46.15	150.8	0.3060	24.008	22.4	1936	1501.3600	10000	0.4752	0.08512	1876.7	1.8767E5	3.384E-3	0.4	1.4	84.008	141.59	120.7
50.46	155.9	0.3237	25.008	22.4	1934	1596.8800	10000	0.4746	0.07954	1996.1	1.9961E5	3.384E-3	0.4	1.4	85.008	154.82	124.7
53.10	161.3	0.3291	25.996	22.4	1933	1710.9100	10000	0.4744	0.07427	2138.6	2.1386E5	3.383E-3	0.4	1.4	85.996	162.90	129.1
56.94	169.3	0.3363	27.000	22.4	1927	1886.9301	10000	0.4729	0.06721	2358.7	2.3587E5	3.384E-3	0.5	1.5	87.000	174.70	135.5
59.79	174.4	0.3427	27.996	22.4	1925	1995.6801	10000	0.4725	0.06327	2494.6	2.4946E5	3.384E-3	0.5	1.5	87.996	183.43	139.6
63.42	179.6	0.3532	29.020	22.4	1915	2115.9800	10000	0.4701	0.05941	2645.0	2.6450E5	3.383E-3	0.5	1.5	89.020	194.57	143.6
68.75	187.5	0.3666	30.012	22.4	1918	2305.7700	10000	0.4707	0.05453	2882.2	2.8822E5	3.383E-3	0.5	1.5	90.012	210.92	150.0
70.82	192.7	0.3675	31.012	22.4	1912	2432.1699	10000	0.4693	0.05150	3040.2	3.0402E5	3.384E-3	0.5	1.5	91.012	217.28	154.2
73.41	200.5	0.3661	32.012	22.4	1903	2635.1499	10000	0.4671	0.04733	3293.9	3.2939E5	3.384E-3	0.5	1.5	92.012	225.23	160.4
78.99	205.8	0.3838	32.996	22.4	1894	2773.5500	10000	0.4648	0.04470	3466.9	3.4669E5	3.384E-3	0.5	1.5	92.996	242.33	164.7
81.39	211.0	0.3858	34.000	22.4	1907	2913.2900	10000	0.4681	0.04284	3641.6	3.6416E5	3.384E-3	0.6	1.6	94.000	249.70	168.8
86.23	218.6	0.3945	35.000	22.4	1889	3127.4399	10000	0.4636	0.03953	3909.3	3.9093E5	3.384E-3	0.6	1.6	95.000	264.55	174.9
91.22	223.9	0.4074	36.012	22.4	1875	3279.0601	10000	0.4602	0.03740	4098.8	4.0988E5	3.384E-3	0.6	1.6	96.012	279.85	179.1
93.78	229.1	0.4094	36.996	22.4	1876	3430.8000	10000	0.4604	0.03574	4288.5	4.2885E5	3.384E-3	0.6	1.6	96.996	287.70	183.3
99.14	236.6	0.4190	37.996	22.4	1875	3658.0500	10000	0.4602	0.03348	4572.6	4.5726E5	3.383E-3	0.6	1.6	97.996	304.15	189.3
102.8	241.8	0.4253	39.000	22.4	1876	3822.4199	10000	0.4606	0.03209	4778.0	4.7780E5	3.383E-3	0.7	1.7	99.000	315.53	193.5
108.1	249.6	0.4330	40.012	22.4	1867	4069.0100	10000	0.4581	0.02997	5086.3	5.0863E5	3.383E-3	0.7	1.7	100.012	331.57	199.7
111.5	254.6	0.4379	41.020	22.4	1860	4232.7598	10000	0.4565	0.02869	5291.0	5.2910E5	3.384E-3	0.7	1.7	101.020	342.09	203.7
116.2	259.8	0.4472	42.004	22.4	1864	4499.3198	10000	0.4575	0.02761	5624.2	5.6242E5	3.384E-3	0.7	1.7	102.004	356.51	207.9
120.7	267.6	0.4510	42.996	22.4	1857	4678.7598	10000	0.4557	0.02593	5848.5	5.8485E5	3.383E-3	0.7	1.7	102.996	370.28	214.1
123.3	272.7	0.4523	44.000	22.4	1852	4851.2402	10000	0.4545	0.02491	6064.1	6.0641E5	3.384E-3	0.7	1.7	104.000	378.34	218.1
129.3	280.3	0.4614	45.024	22.4	1847	5128.8701	10000	0.4533	0.02350	6411.1	6.4111E5	3.384E-3	0.8	1.8	105.024	396.82	224.3
133.4	285.5	0.4673	45.996	22.4	1843	5318.2798	10000	0.4524	0.02261	6647.9	6.6479E5	3.384E-3	0.8	1.8	105.996	409.32	228.4
137.9	293.1	0.4706	47.008	22.4	1837	5603.2100	10000	0.4508	0.02138	7004.0	7.0040E5	3.384E-3	0.8	1.8	107.008	423.18	234.5
142.5	298.1	0.4780	48.012	22.4	1823	5797.7202	10000	0.4474	0.02051	7247.2	7.2472E5	3.383E-3	0.8	1.8	108.012	437.17	238.5
146.0	303.3	0.4813	49.004	22.4	1824	5999.5601	10000	0.4476	0.01982	7499.5	7.4995E5	3.383E-3	0.8	1.8	109.004	447.92	242.7
153.2	311.0	0.4928	49.996	22.4	1836	6302.2900	10000	0.4506	0.01899	7877.9	7.8779E5	3.383E-3	0.8	1.8	109.996	470.16	248.8
156.0	316.0	0.4938	50.996	22.4	1838	6510.5601	10000	0.4510	0.01840	8138.2	8.1382E5	3.383E-3	0.8	1.8	110.996	478.72	252.8
162.1	323.8	0.5005	52.012	22.4	1827	6832.2100	10000	0.4484	0.01743	8540.3	8.5403E5	3.384E-3	0.9	1.9	112.012	497.21	259.0
162.3	328.9	0.4934	52.996	22.4	1827	7046.6499	10000	0.4484	0.01689	8808.3	8.8083E5	3.384E-3	0.9	1.9	112.996	497.83	263.1
168.2	336.4	0.5001	54.012	22.4	1815	7380.2100	10000	0.4453	0.01603	9225.3	9.2253E5	3.384E-3	0.9	1.9	114.012	516.17	269.1
177.4	341.6	0.5195	55.012	22.4	1818	7602.8701	10000	0.4462	0.01558	9503.6	9.5036E5	3.384E-3	0.9	1.9	115.012	544.38	273.3
176.0	346.7	0.5077	56.012	22.4	1820	7828.3101	10000	0.4468	0.01514	9785.4	9.7854E5	3.384E-3	0.9	1.9	116.012	540.00	277.4
186.3	354.2	0.5261	56.996	22.4	1797	8170.5000	10000	0.4411	0.01433	10213	1.0213E6	3.383E-3	0.9	1.9	116.996	571.71	283.4
191.0	359.3	0.5316	57.996	22.4	1784	8408.6396	10000	0.4378	0.01382	10511	1.0511E6	3.383E-3	1.0	2.0	117.996	586.06	287.5
193.5	367.0	0.5274	59.004	22.4	1786	8768.5195	10000	0.4384	0.01326	10961	1.0961E6	3.384E-3	1.0	2.0	119.004	593.79	293.6
202.0	372.0	0.5430	60.012	22.4	1779	9014.0801	10000	0.4366	0.01286	11268	1.1268E6	3.383E-3	1.0	2.0	120.012	619.78	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

207.6	375.0	0.5537	0.99600	22.4	1745	286.3070	10000	0.4283	0.01241	357.88	35788	3.383E-3	0.0	2.0	121.996	637.03	300.0
204.8	375.0	0.5461	1.9920	22.4	1762	537.3870	10000	0.4326	0.01253	671.73	67173	3.383E-3	0.0	2.0	122.992	628.23	300.0
208.1	375.0	0.5549	3.0000	22.4	1742	914.3770	10000	0.4275	0.01239	1143.0	1.1430E5	3.383E-3	0.1	2.1	124.000	638.43	300.0
208.0	375.0	0.5546	3.9920	22.4	1762	1165.8199	10000	0.4326	0.01253	1457.3	1.4573E5	3.383E-3	0.1	2.1	124.992	638.09	300.0
205.0	375.0	0.5466	4.9920	22.4	1766	1416.9500	10000	0.4334	0.01256	1771.2	1.7712E5	3.383E-3	0.1	2.1	125.992	628.81	300.0
203.3	375.0	0.5422	5.9920	22.4	1795	1795.1899	10000	0.4405	0.01276	2244.0	2.2440E5	3.384E-3	0.1	2.1	126.992	623.85	300.0
203.0	375.0	0.5414	7.0120	22.4	1795	2049.1001	10000	0.4407	0.01277	2561.4	2.5614E5	3.384E-3	0.1	2.1	128.012	622.86	300.0
203.8	375.0	0.5433	7.9960	22.4	1772	2426.4600	10000	0.4348	0.01260	3033.1	3.0331E5	3.384E-3	0.1	2.1	128.996	625.11	300.0
204.3	375.0	0.5448	9.0120	22.4	1801	2675.9500	10000	0.4421	0.01281	3344.9	3.3449E5	3.384E-3	0.2	2.2	130.012	626.83	300.0
203.8	375.0	0.5435	10.016	22.4	1800	2926.3601	10000	0.4417	0.01280	3658.0	3.6580E5	3.384E-3	0.2	2.2	131.016	625.32	300.0
201.9	375.0	0.5385	11.012	22.4	1779	3305.5601	10000	0.4366	0.01265	4132.0	4.1320E5	3.383E-3	0.2	2.2	132.012	619.53	300.0
205.7	375.0	0.5486	12.008	22.4	1768	3554.7400	10000	0.4340	0.01257	4443.4	4.4434E5	3.384E-3	0.2	2.2	133.008	631.17	300.0
202.7	375.0	0.5405	13.008	22.4	1781	3829.6299	10000	0.4370	0.01266	4787.0	4.7870E5	3.384E-3	0.2	2.2	134.008	621.81	300.0
204.0	375.0	0.5439	13.992	22.4	1754	4181.7002	10000	0.4305	0.01247	5227.1	5.2271E5	3.384E-3	0.2	2.2	134.992	625.77	300.0
206.9	375.0	0.5517	14.992	22.4	1773	4434.1699	10000	0.4352	0.01261	5542.7	5.5427E5	3.383E-3	0.2	2.3	135.992	634.69	300.0
202.8	375.0	0.5407	16.000	22.4	1758	4809.9399	10000	0.4315	0.01250	6012.4	6.0124E5	3.383E-3	0.3	2.3	137.000	622.11	300.0
205.9	375.0	0.5491	16.992	22.4	1769	5061.3398	10000	0.4342	0.01258	6326.7	6.3267E5	3.383E-3	0.3	2.3	137.992	631.66	300.0
202.4	375.0	0.5397	17.992	22.4	1782	5313.6899	10000	0.4374	0.01267	6642.1	6.6421E5	3.383E-3	0.3	2.3	138.992	620.96	300.0
203.2	375.0	0.5419	18.996	22.4	1784	5689.6499	10000	0.4378	0.01269	7112.1	7.1121E5	3.383E-3	0.3	2.3	139.996	623.43	300.0
205.2	375.0	0.5473	19.992	22.4	1777	5940.7998	10000	0.4362	0.01264	7426.0	7.4260E5	3.383E-3	0.3	2.3	140.992	629.67	300.0
208.8	375.0	0.5569	20.992	22.4	1782	6319.3999	10000	0.4374	0.01267	7899.3	7.8993E5	3.384E-3	0.3	2.4	141.992	640.73	300.0
205.3	375.0	0.5476	21.996	22.4	1779	6569.1802	10000	0.4366	0.01265	8211.5	8.2115E5	3.384E-3	0.4	2.4	142.996	629.94	300.0
203.8	375.0	0.5435	22.996	22.4	1787	6821.2402	10000	0.4387	0.01271	8526.6	8.5266E5	3.383E-3	0.4	2.4	143.996	625.27	300.0
203.5	375.0	0.5426	23.992	22.4	1789	7197.4199	10000	0.4391	0.01272	8996.8	8.9968E5	3.384E-3	0.4	2.4	144.992	624.27	300.0
203.2	375.0	0.5419	25.016	22.4	1763	7450.1499	10000	0.4328	0.01254	9312.7	9.3127E5	3.384E-3	0.4	2.4	146.016	623.46	300.0
203.0	375.0	0.5414	25.996	22.4	1758	7702.0898	10000	0.4315	0.01250	9627.6	9.6276E5	3.383E-3	0.4	2.4	146.996	622.91	300.0
205.6	375.0	0.5483	26.996	22.4	1791	8077.2998	10000	0.4397	0.01274	10097	1.0097E6	3.384E-3	0.4	2.5	147.996	630.80	300.0
204.8	375.0	0.5462	28.008	22.4	1783	8328.4902	10000	0.4376	0.01268	10411	1.0411E6	3.384E-3	0.5	2.5	149.008	628.35	300.0
203.3	375.0	0.5421	29.012	22.4	1781	8705.5400	10000	0.4372	0.01267	10882	1.0882E6	3.384E-3	0.5	2.5	150.012	623.72	300.0
202.2	375.0	0.5392	30.020	22.4	1796	8956.8096	10000	0.4409	0.01277	11196	1.1196E6	3.384E-3	0.5	2.5	151.020	620.33	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

205.4	370.6	0.5543	0.99600	22.4	1779	296.0530	10000	0.4366	0.01295	370.07	37007	3.384E-3	0.0	2.5	151.996	630.23	296.5
197.1	365.6	0.5391	2.0000	22.4	1783	534.3140	10000	0.4376	0.01334	667.89	66789	3.384E-3	0.0	2.6	153.000	604.65	292.5
191.4	358.0	0.5346	3.0240	22.4	1797	894.0890	10000	0.4411	0.01403	1117.6	1.1176E5	3.384E-3	0.1	2.6	154.024	587.07	286.4
185.2	352.8	0.5249	4.0080	22.4	1823	1129.1500	10000	0.4474	0.01465	1411.4	1.4114E5	3.384E-3	0.1	2.6	155.008	568.16	282.2
184.6	347.7	0.5310	4.9960	22.4	1804	1356.4000	10000	0.4427	0.01492	1695.5	1.6955E5	3.384E-3	0.1	2.6	155.996	566.47	278.2
175.1	340.1	0.5148	6.0080	22.4	1809	1692.6600	10000	0.4439	0.01564	2115.8	2.1158E5	3.383E-3	0.1	2.6	157.008	537.14	272.1
169.0	335.0	0.5045	6.9960	22.4	1804	1918.0100	10000	0.4427	0.01608	2397.5	2.3975E5	3.383E-3	0.1	2.6	157.996	518.41	268.0
166.5	327.4	0.5086	8.0120	22.4	1789	2247.2700	10000	0.4391	0.01669	2809.1	2.8091E5	3.384E-3	0.1	2.7	159.012	510.92	261.9
163.6	322.4	0.5075	8.9960	22.4	1815	2450.1201	10000	0.4453	0.01746	3062.7	3.0627E5	3.383E-3	0.1	2.7	159.996	501.91	257.9
156.1	314.6	0.4963	9.9920	22.4	1806	2769.3899	10000	0.4433	0.01825	3461.7	3.4617E5	3.383E-3	0.2	2.7	160.992	479.02	251.7
153.4	309.6	0.4956	10.996	22.4	1808	2969.7300	10000	0.4437	0.01887	3712.2	3.7122E5	3.383E-3	0.2	2.7	161.996	470.73	247.7
147.3	302.0	0.4879	12.020	22.4	1831	3270.2700	10000	0.4494	0.02008	4087.8	4.0878E5	3.384E-3	0.2	2.7	163.020	451.97	241.6
137.9	296.8	0.4645	12.992	22.4	1871	3477.1299	10000	0.4591	0.02124	4346.4	4.3464E5	3.383E-3	0.2	2.7	163.992	422.97	237.4
136.9	291.6	0.4694	13.996	22.4	1857	3664.4500	10000	0.4559	0.02184	4580.6	4.5806E5	3.383E-3	0.2	2.7	164.996	419.92	233.3
134.1	284.0	0.4720	15.012	22.4	1838	3945.8601	10000	0.4512	0.02279	4932.3	4.9323E5	3.384E-3	0.3	2.8	166.012	411.30	227.2
130.1	278.9	0.4665	16.012	22.4	1839	4133.5898	10000	0.4514	0.02365	5167.0	5.1670E5	3.384E-3	0.3	2.8	167.012	399.13	223.1
124.1	271.2	0.4576	17.000	22.4	1855	4404.4600	10000	0.4553	0.02522	5505.6	5.5056E5	3.383E-3	0.3	2.8	168.000	380.77	217.0
117.0	266.2	0.4397	17.996	22.4	1883	4578.7002	10000	0.4622	0.02658	5723.4	5.7234E5	3.383E-3	0.3	2.8	168.996	359.10	213.0
116.2	261.1	0.4452	18.992	22.4	1867	4752.8999	10000	0.4581	0.02739	5941.1	5.9411E5	3.383E-3	0.3	2.8	169.992	356.53	208.8
109.9	253.2	0.4338	19.996	22.4	1862	5010.1401	10000	0.4569	0.02903	6262.7	6.2627E5	3.384E-3	0.3	2.8	170.996	337.03	202.6
106.8	248.2	0.4301	20.996	22.4	1876	5171.9102	10000	0.4604	0.03044	6464.9	6.4649E5	3.384E-3	0.3	2.9	171.996	327.54	198.6
100.8	240.5	0.4192	21.996	22.4	1863	5415.6499	10000	0.4573	0.03221	6769.6	6.7696E5	3.383E-3	0.4	2.9	172.996	309.34	192.4
97.60	235.2	0.4149	23.012	22.4	1911	5578.9800	10000	0.4691	0.03455	6973.7	6.9737E5	3.384E-3	0.4	2.9	174.012	299.44	188.2
94.22	230.1	0.4094	24.012	22.4	1885	5804.2500	10000	0.4626	0.03559	7255.3	7.2553E5	3.383E-3	0.4	2.9	175.012	289.05	184.1
90.65	222.4	0.4075	25.012	22.4	1876	5953.1802	10000	0.4604	0.03791	7441.5	7.4415E5	3.384E-3	0.4	2.9	176.012	278.10	177.9
85.34	217.2	0.3930	25.996	22.4	1883	6104.2700	10000	0.4622	0.03993	7630.3	7.6303E5	3.384E-3	0.4	2.9	176.996	261.81	173.7
80.71	209.6	0.3851	26.996	22.4	1904	6309.3501	10000	0.4673	0.04335	7886.7	7.8867E5	3.384E-3	0.4	3.0	177.996	247.60	167.7
77.96	204.4	0.3813	28.000	22.4	1908	6446.8101	10000	0.4683	0.04565	8058.5	8.0585E5	3.384E-3	0.5	3.0	179.000	239.17	163.5
74.87	199.2	0.3759	29.012	22.4	1912	6584.1602	10000	0.4693	0.04820	8230.2	8.2302E5	3.383E-3	0.5	3.0	180.012	229.68	159.3
72.34	191.4	0.3781	29.996	22.4	1915	6777.6699	10000	0.4701	0.05231	8472.1	8.4721E5	3.384E-3	0.5	3.0	180.996	221.95	153.1
68.30	186.3	0.3667	30.996	22.4	1909	6902.6001	10000	0.4685	0.05502	8628.3	8.6283E5	3.384E-3	0.5	3.0	181.996	209.53	149.0
62.57	178.3	0.3509	32.200	22.4	1921	7089.7402	10000	0.4715	0.06042	8862.2	8.8622E5	3.384E-3	0.5	3.1	183.200	191.96	142.7
59.11	173.0	0.3418	32.996	22.4	1929	7208.2598	10000	0.4735	0.06450	9010.3	9.0103E5	3.384E-3	0.5	3.1	183.996	181.35	138.4
56.19	167.9	0.3348	34.012	22.4	1934	7322.4199	10000	0.4748	0.06865	9153.0	9.1530E5	3.384E-3	0.6	3.1	185.012	172.39	134.3
51.44	159.9	0.3217	35.012	22.4	1927	7488.8599	10000	0.4729	0.07535	9361.1	9.3611E5	3.384E-3	0.6	3.1	186.012	157.82	127.9
50.32	154.5	0.3256	36.008	22.4	1920	7595.7100	10000	0.4713	0.08040	9494.6	9.4946E5	3.383E-3	0.6	3.1	187.008	154.39	123.6
47.59	149.5	0.3184	36.996	22.4	1935	7694.5898	10000	0.4750	0.08663	9618.2	9.6182E5	3.383E-3	0.6	3.1	187.996	146.00	119.6
43.05	141.5	0.3042	37.996	22.4	1929	7844.1201	10000	0.4733	0.09630	9805.2	9.8052E5	3.383E-3	0.6	3.1	188.996	132.08	113.2
40.58	136.1	0.2981	38.996	22.4	1943	7937.5200	10000	0.4770	0.1049	9921.9	9.9219E5	3.384E-3	0.6	3.2	189.996	124.49	108.9
37.36	131.1	0.2850	40.000	22.4	1929	8024.6401	10000	0.4735	0.1123	10031	1.0031E6	3.384E-3	0.7	3.2	191.000	114.63	104.9
34.17	123.1	0.2775	41.012	22.4	1943	8155.3799	10000	0.4770	0.1282	10194	1.0194E6	3.384E-3	0.7	3.2	192.012	104.84	98.51
31.45	117.5	0.2676	41.996	22.4	1939	8242.3496	10000	0.4760	0.1404	10303	1.0303E6	3.384E-3	0.7	3.2	192.996	96.491	94.03
28.95	112.3	0.2577	42.996	22.4	1942	8318.0996	10000	0.4766	0.1539	10398	1.0398E6	3.384E-3	0.7	3.2	193.996	88.803	89.85
26.23	104.3	0.2514	43.996	22.4	1943	8428.6797	10000	0.4770	0.1786	10536	1.0536E6	3.384E-3	0.7	3.2	194.996	80.468	83.46
23.77	98.65	0.2409	45.000	22.4	1952	8503.2500	10000	0.4790	0.2006	10629	1.0629E6	3.384E-3	0.8	3.3	196.000	72.916	78.92
21.65	93.40	0.2318	45.996	22.4	1963	8565.1201	10000	0.4819	0.2250	10706	1.0706E6	3.384E-3	0.8	3.3	196.996	66.426	74.72
19.50	88.11	0.2213	47.016	22.4	1967	8627.3203	10000	0.4827	0.2533	10784	1.0784E6	3.384E-3	0.8	3.3	198.016	59.826	70.49
16.81	79.55	0.2113	48.024	22.4	1973	8719.7803	10000	0.4843	0.3118	10900	1.0900E6	3.384E-3	0.8	3.3	199.024	51.560	63.64
14.90	74.27	0.2007	48.996	22.4	1960	8769.2197	10000	0.4811	0.3554	10962	1.0962E6	3.384E-3	0.8	3.3	199.996	45.724	59.41
13.02	68.93	0.1889	50.008	22.4	1972	8818.6396	10000	0.4841	0.4152	11023	1.1023E6	3.384E-3	0.8	3.4	201.008	39.944	55.14
11.61	63.15	0.1839	50.996	22.4	1971	8867.7900	10000	0.4837	0.4941	11085	1.1085E6	3.383E-3	0.8	3.4	201.996	35.628	50.52
8.894	54.69	0.1626	52.000	22.4	1960	8929.1602	10000	0.4811	0.6553	11161	1.1161E6	3.383E-3	0.9	3.4	203.000	27.288	43.75
7.513	49.20	0.1527	53.012	22.4	1972	8965.9004	10000	0.4839	0.8143	11207	1.1207E6	3.383E-3	0.9	3.4	204.012	23.051	39.36
5.887	43.07	0.1367	53.996	22.4	1976	9002.5098	10000	0.4849	1.065	11253	1.1253E6	3.384E-3	0.9	3.4	204.996	18.063	34.46
4.504	36.62	0.1230	55.000	22.4	1977	9032.5703	10000	0.4853	1.474	11291	1.1291E6	3.384E-3	0.9	3.4	206.000	13.817	29.30
3.477	31.09	0.1119	56.012	22.4	1980	9056.6699	10000	0.4859	2.049	11321	1.1321E6	3.383E-3	0.9	3.5	207.012	10.669	24.87
2.332	24.44	0.09543	56.996	22.4	1976	9080.2803	10000	0.4849	3.309	11350	1.1350E6	3.383E-3	0.9	3.5	207.996	7.1541	19.55
1.741	20.42	0.08525	57.996	22.4	1972	9091.7100	10000	0.4841	4.731	11365	1.1365E6	3.383E-3	1.0	3.5	208.996	5.3403	16.33
1.053	14.01	0.07516	58.996	22.4	1977	9103.1699	10000	0.4851	10.07	11379	1.1379E6	3.383E-3	1.0	3.5	209.996	3.2302	11.21
0.3751	7.064	0.05310	60.004	22.4	1969	9111.0898	10000	0.4833	39.46	11389	1.1389E6	3.383E-3	1.0	3.5	211.004	1.1508	5.651

